Labconco FreeZone 4.5 Liter Freeze Dry Systems 77510 Series User Manual

FreeZone 4.5 Liter Freeze Dry Systems Models 77500 Series 77510 Series User’s Manual Labconco Corporation 8811 Prospect Avenue

Product Service 1-800-522-7658 6 CCHHAAPPTTEERR 22 PPRREERREEQQUUIISSIITTEESS Before you install your Freeze Dryer, you need to prepare y

Chapter 2: Prerequisites Product Service 1-800-522-7658 7 IT IS RECOMMENDED THAT THE CONSOLE MODEL FREEZE DRYER BE SECURELY ATTACHED TO THE FLOOR AFT

Product Service 1-800-522-7658 8 CCHHAAPPTTEERR 33 GGEETTTTIINNGG SSTTAARRTTEEDD Now that the site for your Freeze Dryer is properly pr

Chapter 3: Getting Started Product Service 1-800-522-7658 9 DO NOT DISCARD THE CARTON OR PACKING MATERIAL FOR YOUR FREEZE DRYER UNTIL YOU HAVE CHECKE

Chapter 3: Getting Started Product Service 1-800-522-7658 10 Plus the following: Part # Component Description 7416600 User’s Manual 1291000 Plug (2

Chapter 3: Getting Started Product Service 1-800-522-7658 11 Vacuum Pump Connection A vacuum pump as described in Chapter 2: Prerequisites is requi

Chapter 3: Getting Started Product Service 1-800-522-7658 12 Acids Buffers Solvents Component Material Acetic Acid 20% Formic Acid Trifluoroacet

Chapter 3: Getting Started Product Service 1-800-522-7658 13  Rubber and plastic components that have been exposed to damaging compounds should be

Product Service 1-800-522-7658 14 CCHHAAPPTTEERR 44 UUSSIINNGG YYOOUURR FFRREEEEZZEE DDRRYYEERR After your Freeze Dryer has been inst

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 15 Freeze Dryer Controls The control panel for the Freeze Dryer is shown below wit

Copyright © 2004, 2007, 2012, 2013, 2014 Labconco Corporation. All rights reserved. The information contained in this manual and the accompanying p

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 16 11. Collector Temperature Graph Display – This display indicates the temperature

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 17  Press SELECT until the desired units are flashing.  Press MENU.  The dis

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 18  To reset the SERVICE HOUR to 0, press SELECT.  The display will show:

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 19 will show the actual temperature of the collector. When the vacuum in the syste

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 20 containers or larger). The temperature required for pre-freezing is dependent o

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 21 5. Ampules may be flame sealed while connected to a valve by using a sealing to

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 22 Alarms A number of unusual events may occur during a lyophilization procedure t

Chapter 4: Using Your Freeze Dryer Product Service 1-800-522-7658 23 Temperature Out of Range An alarm will be activated if the collector temperatu

Product Service 1-800-522-7658 24 CCHHAAPPTTEERR 55 MMAAIINNTTAAIINNIINNGG YYOOUURR FFRREEEEZZEE DDRRYYEERR Under normal operation, t

Chapter 5: Maintaining Your Freeze Dryer Product Service 1-800-522-7658 25 Monthly: 1. The rubber components on the Freeze Dryer may eventually de

TTAABBLLEE OOFF CCOONNTTEENNTTSS CHAPTER 1: INTRODUCTION 1 Freeze Dry Process 1 Freeze Dry Rates

Product Service 1-800-522-7658 26 CCHHAAPPTTEERR 66 UUSSIINNGG TTHHEE RRSS223322 RREECCEEPPTTAACCLLEE The operation of the Freeze Dry

Chapter 6: Using the RS232 Receptacle Product Service 1-800-522-7658 27 The time between data transmissions may be varied by the user to occur at 10

Chapter 6: Using the RS232 Receptacle Product Service 1-800-522-7658 28 3. The “Connection Description” dialogue box will open. Type in a user defi

Chapter 6: Using the RS232 Receptacle Product Service 1-800-522-7658 29 5. The “Com X Properties” dialogue box will open. Enter the appropriate da

Product Service 1-800-522-7658 30 CCHHAAPPTTEERR 77 TTRROOUUBBLLEESSHHOOOOTTIINNGG Refer to the following if your Freeze Dryer fails t

Chapter 7: Troubleshooting Product Service 1-800-522-7658 31 4. Isolate the pump by disconnecting the vacuum hose from the Freeze Dryer. Deadhead t

Chapter 7: Troubleshooting Product Service 1-800-522-7658 32 The illustrations below show how the sample valve installs on a chamber and a manifold.

Chapter 7: Troubleshooting Product Service 1-800-522-7658 33 III. System Components and Collection Chamber Isolation The following test is used to

Product Service 1-800-522-7658 34 CCHHAAPPTTEERR 88 MMOODDIIFFYYIINNGG YYOOUURR FFRREEEEZZEE DDRRYYEERR DDIISSPPLLAAYY Your Freeze Dryer

Chapter 8: Modifying Your Freeze Dryer Display Product Service 1-800-522-7658 35 Moisture Sensor Alarm The moisture sensor alarm may be disabled. It

Shut Down 21 Defrosting 21 Alarms 22 Power Failure 22 Line Voltage Out of Range

Chapter 8: Modifying Your Freeze Dryer Display Product Service 1-800-522-7658 36 Press MENU and if the drying chamber has been installed, the display

Chapter 8: Modifying Your Freeze Dryer Display Product Service 1-800-522-7658 37 Press MENU and the display will show: Press and hold SELECT to c

Chapter 8: Modifying Your Freeze Dryer Display Product Service 1-800-522-7658 38 In order to store offsets in memory, you Must Press and Hold MENU un

Product Service 1-800-522-7658 39 AAPPPPEENNDDIIXX AA FFRREEEEZZEE DDRRYYEERR CCOOMMPPOONNEENNTTSS The following pages list components tha

Appendix A: Freeze Dryer Components Product Service 1-800-522-7658 40 Item Part No. Description 1 7688500 Lid Gasket 2 7730700 Lid 3 7448000 Prin

Appendix A: Freeze Dryer Components Product Service 1-800-522-7658 41

Product Service 1-800-522-7658 42 AAPPPPEENNDDIIXX BB FFRREEEEZZEE DDRRYYEERR DDIIMMEENNSSIIOONNSS Model 77500xx

Appendix B: Freeze Dryer Dimensions Product Service 1-800-522-7658 43 Model 77510xx

Product Service 816-333-8811 or 1-800-522-7658 44 AAPPPPEENNDDIIXX CC FFRREEEEZZEE DDRRYYEERR SSPPEECCIIFFIICCAATTIIOONNSS This Appendix co

Appendix C: Freeze Dryer Specifications Product Service 1-800-522-7658 45 Environmental Conditions  Indoor use only.  Maximum altitude: 6562 f

Product Service 1-800-522-7658 1 CCHHAAPPTTEERR 11 IINNTTRROODDUUCCTTIIOONN Congratulations on your purchase of a Labconco FreeZone® Free

Product Service 816-333-8811 or 1-800-522-7658 46 AAPPPPEENNDDIIXX DD FFRREEEEZZEE DDRRYYEERR AACCCCEESSSSOORRIIEESS PART # DESCRIPTION

Appendix D: Freeze Dryer Accessories Product Service 1-800-522-7658 47 PART # DESCRIPTION 1472200 Pump Inlet Filter Disposable filter that prevents

Appendix D: Freeze Dryer Accessories Product Service 1-800-522-7658 48 PART # DESCRIPTION 7522800 12 Port Drying Chamber 9 ¾" high x 7 7/8&qu

Appendix D: Freeze Dryer Accessories Product Service 1-800-522-7658 49 Fast-Freeze® Flasks

Appendix D: Freeze Dryer Accessories Product Service 1-800-522-7658 50 Lyph-Lock® Flasks

Appendix D: Freeze Dryer Accessories Product Service 1-800-522-7658 51 Serum Bottles & Vials

Appendix D: Freeze Dryer Accessories Product Service 1-800-522-7658 52 Ampules

Chapter 1: Introduction Product Service 1-800-522-7658 2 A listing of selected materials and their approximate drying times are shown in Table 1 for

Chapter 1: Introduction Product Service 1-800-522-7658 3 The rate of freeze drying is directly proportional to the vapor pressure and the vapor pres

Chapter 1: Introduction Product Service 1-800-522-7658 4 Samples Containing Volatile Substances In certain cases the solvent in a sample to be freeze

Chapter 1: Introduction Product Service 1-800-522-7658 5 Appendix A: Freeze Dryer Components contains labeled diagrams of the components of the Free