Labconco FreeZone 6 Liter Benchtop Freeze Dry Systems 77520 User Manual

FreeZone® 6 Liter BenchtopFreeze Dry SystemsModels 77520 Series User’s ManualLabconco Corporation 8811 Prospect Avenue Kansas City

6 Product Service: Domestic 1-800-522-7658, International 816-333-8811 Chapter 1: Introduction Typographical Conventions Recognizing the followi

7 Product Service: Domestic 1-800-522-7658, International 816-333-8811 CCHHAAPPTTEERR 22 PPRREERREEQQUUIISSIITTEESS Before you inst

8 Chapter 2: Prerequisites Product Service: Domestic 1-800-522-7658, International 816-333-8811 Location Requirements The Freeze Dryer should be

9 Product Service: Domestic 1-800-522-7658, International 816-333-8811 CCHHAAPPTTEERR 33 GGEETTTTIINNGG SSTTAARRTTEEDD Now that th

10 Chapter 3: Getting Started Product Service: Domestic 1-800-522-7658, International 816-333-8811 IF YOUR FREEZE DRYER WAS DAMAGED IN TRANSIT,

11 Chapter 3: Getting Started Product Service: Domestic 1-800-522-7658, International 816-333-8811 Setting Up Your Freeze Dryer After you verif

12 Chapter 3: Getting Started Product Service: Domestic 1-800-522-7658, International 816-333-8811 Chemical Resistance of Freeze Dryer Component

13 Chapter 3: Getting Started Product Service: Domestic 1-800-522-7658, International 816-333-8811 When using compounds in the Freeze Dryer tha

14 Chapter 3: Getting Started Product Service: Domestic 1-800-522-7658, International 816-333-8811 Hazardous materials such as strong acids or b

15 Product Service: Domestic 1-800-522-7658, International 816-333-8811 CCHHAAPPTTEERR 44 UUSSIINNGG YYOOUURR FFRREEEEZZEE DDRRYYEE

Copyright © 2004, 2007, 2012, 2013 Labconco Corporation. All rights reserved. The information contained in this manual and the accompanying products

16 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 Freeze Dryer Controls The control pan

17 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 9. Auto Mode Indicator – When lit,

18 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 5. Inspect each sample valve on the

19 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 • Press SELECT until the desired va

20 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 • To reset the SERVICE HOUR to 0, pr

21 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 Manual Start-Up To manually run the

22 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 Some guidelines for setting the Freez

23 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 2. Before adding another sample

24 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 Shut Down At the end of a run or when

25 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 Alarms A number of unusual events ma

TTAABBLLEE OOFF CCOONNTTEENNTTSS CHAPTER 1: INTRODUCTION 1 Freeze Dry Process 1 Freeze Dry Rates 2 Freeze Dry Capaci

26 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 Line Voltage Out of Range If the vol

27 Chapter 4: Using Your Freeze Dryer Product Service: Domestic 1-800-522-7658, International 816-333-8811 Moisture in Collector If there is l

28 Product Service: Domestic 1-800-522-7658, International 816-333-8811 CCHHAAPPTTEERR 55 MMAAIINNTTAAIINNIINNGG YYOOUURR FFRREEEEZZ

29 Chapter 5: Maintaining Your RapidVap Product Service: Domestic 1-800-522-7658, International 816-333-8811 Monthly: 1. The rubber components

30 Product Service: Domestic 1-800-522-7658, International 816-333-8811 CCHHAAPPTTEERR 66 UUSSIINNGG TTHHEE RRSS223322 RREECCEEPPTTAA

31 Chapter 6: Using the RS232 Receptacle Product Service: Domestic 1-800-522-7658, International 816-333-8811 1. Data Rate 2400 Baud 2. 8 Bit

32 Chapter 6: Using the RS232 Receptacle Product Service: Domestic 1-800-522-7658, International 816-333-8811 following describes how to use an

33 Chapter 6: Using the RS232 Receptacle Product Service: Domestic 1-800-522-7658, International 816-333-8811 5. The “Com X Properties” dialo

34 Chapter 6: Using the RS232 Receptacle Product Service: Domestic 1-800-522-7658, International 816-333-8811 6. When the Freeze Dryer main pow

35 Product Service: Domestic 1-800-522-7658, International 816-333-8811 CCHHAAPPTTEERR 77 TTRROOUUBBLLEESSHHOOOOTTIINNGG Refer to th

Defrosting 24 Alarms 25 Power Failure 25 Line Voltage Out of Range 26 Temperature Out of Range 26 Service Vacuum Pump

36 Chapter 7: Troubleshooting Product Service: Domestic 1-800-522-7658, International 816-333-8811 If vacuum problems continue, consider obtaini

37 Chapter 7: Troubleshooting Product Service: Domestic 1-800-522-7658, International 816-333-8811 7. Make sure that the sample valve bulkhead

38 Chapter 7: Troubleshooting Product Service: Domestic 1-800-522-7658, International 816-333-8811 III. System Componen

39 Chapter 7: Troubleshooting Product Service: Domestic 1-800-522-7658, International 816-333-8811 The following test allows you to check the

40 Chapter 7: Troubleshooting Product Service: Domestic 1-800-522-7658, International 816-333-8811 The following test is used to check the colle

41 Chapter 7: Troubleshooting Product Service: Domestic 1-800-522-7658, International 816-333-8811 4. If bubbling was observed on the chamber

42 Product Service Domestic 1-800-522-7658, International 816-333-8811 CCHHAAPPTTEERR 88 MMOODDIIFFYYIINNGG YYOOUURR FFRREEEEZZEE DDRRYYE

43 Chapter 8: Modifying Your Freeze Dryer Display Product Service: Domestic 1-800-522-7658, International 816-333-8811 Low line limit may be low

44 Chapter 8: Modifying Your Freeze Dryer Display Product Service: Domestic 1-800-522-7658, International 816-333-8811 The display will default

45 Chapter 8: Modifying Your Freeze Dryer Display Product Service: Domestic 1-800-522-7658, International 816-333-8811 Press SELECT until the a

1 Product Service: Domestic 1-800-522-7658, International 816-333-8811 CCHHAAPPTTEERR 11 IINNTTRROODDUUCCTTIIOONN Congratulations on

46 Chapter 8: Modifying Your Freeze Dryer Display Product Service: Domestic 1-800-522-7658, International 816-333-8811 Press MENU and the displ

47 Product Service Domestic 1-800-522-7658, International 816-333-8811 AAPPPPEENNDDIIXX AA FFRREEEEZZEE DDRRYYEERR CCOOMMPPOONNEENNTTSS

48 Appendix A: Freeze Dryer Components Product Service: Domestic 1-800-522-7658, International 816-333-8811 Item Part No. Description 1 7690

49 Appendix A: Freeze Dryer Components Product Service: Domestic 1-800-522-7658, International 816-333-8811

50 Product Service Domestic 1-800-522-7658, International 816-333-8811 AAPPPPEENNDDIIXX BB FFRREEEEZZEE DDRRYYEERR DDIIMMEENNSSIIOONNSS

51 Product Service Domestic 1-800-522-7658, International 816-333-8811 AAPPPPEENNDDIIXX CC FFRREEEEZZEE DDRRYYEERR SSPPEECCIIFFIICCAATTI

52 Appendix C: Freeze Dryer Specifications Product Service: Domestic 1-800-522-7658, International 816-333-8811 Environmental Conditions • I

53 Product Service Domestic 1-800-522-7658, International 816-333-8811 AAPPPPEENNDDIIXX DD FFRREEEEZZEE DDRRYYEERR AACCCCEESSSSOORRIIEESS

54 Appendix D: Freeze Dryer Accessories Product Service: Domestic 1-800-522-7658, International 816-333-8811 PART # DESCRIPTION 1473400 Pump Ex

55 Appendix D: Freeze Dryer Accessories Product Service: Domestic 1-800-522-7658, International 816-333-8811 PART # DESCRIPTION 7867000 Clear

2 Product Service: Domestic 1-800-522-7658, International 816-333-8811 Chapter 1: Introduction ice and the heat removed from the collector to co

56 Appendix D: Freeze Dryer Accessories Product Service: Domestic 1-800-522-7658, International 816-333-8811 PART # DESCRIPTION 7509401 Product

57 Appendix D: Freeze Dryer Accessories Product Service: Domestic 1-800-522-7658, International 816-333-8811 PART # DESCRIPTION 7537800 Cable

58 Appendix D: Freeze Dryer Accessories Product Service: Domestic 1-800-522-7658, International 816-333-8811 Fast-Freeze® Flasks

59 Appendix D: Freeze Dryer Accessories Product Service: Domestic 1-800-522-7658, International 816-333-8811 Lyph-Lock® Flasks

60 Appendix D: Freeze Dryer Accessories Product Service: Domestic 1-800-522-7658, International 816-333-8811 Serum Bottles & Vials

61 Appendix D: Freeze Dryer Accessories Product Service: Domestic 1-800-522-7658, International 816-333-8811 Ampules

62 Product Service Domestic 1-800-522-7658, International 816-333-8811

3 Product Service: Domestic 1-800-522-7658, International 816-333-8811 Chapter 1: Introduction sample. The volume of the freeze dry flask shou

4 Product Service: Domestic 1-800-522-7658, International 816-333-8811 Chapter 1: Introduction pressure and ultimately overloads the collector a

5 Product Service: Domestic 1-800-522-7658, International 816-333-8811 Chapter 1: Introduction Chapter 2: Prerequisites explains what you need